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The effects of Al2O3 on micro-structure and crystallization of oxyfluoride glass are investigated by infrared spectra, Raman spectra and X-ray diffraction analyses. The results show that [AlO4] is connected with [SiO4] units by means of angle connection, thereby forming the basic network of glass. When the content of Al2O3 increases, the structures of monomer and dimer increase in oxide glass matrix. Under the condition, the size of nanocrystals has a minimum value, while the structure of nancrystals is not affected.
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Keywords:
- oxyfluoride glass /
- microstructure /
- crystallization
[1] Wang Y, Ohwaki J 1993 Appl. Phys. Lett. 63 3268
[2] Tikhomirov V K, Driesen K, Görller-Walrand C, Mortier M 2007 Opt. Express 15 9535
[3] Meng J, Zhao L J, Yu H, Tang L Q, Liang Q, Yu X Y, Tang B Q, Su J, Xu J J 2005 Acta Phys. Sin. 54 1442 (in Chinese) [孟婕, 赵丽娟, 余华, 唐莉勤, 梁沁, 禹宣伊, 唐伯权, 苏静, 许京军 2005 54 1442]
[4] Chen D Q, Wang Y S, Yu Y L, Ma E, Liu F 2007 J. Phys. Chem. Solids 68 193
[5] Mysen B O, Virgo D, Kushiro I 1981 Am. Mineral. 66 678
[6] Hatta B, Tomozawa M 2008 J. Non-Cryst. Solids 354 3184
[7] Song S X, Chen J S, Zhen W H, Deng W 2009 Glass Enamel 37 5 (in Chinese) [宋树欣, 程金树, 郑伟宏, 邓炜 2009 玻璃与搪瓷 37 5]
[8] Gan F X 1992 Optical and Spectroscopic Properties of Glass (Shanghai: Shanghai Scientific and Technical Publishers) pp39--54 (in Chinese) [干福熹 1992 玻璃的光学和光谱性质(上海:上海科学技术出版社) 第39---54页]
[9] Herzberg G (translated by Wang D C) 1986 Molecular Spectra and Molecular Structure II Infrared and Raman Spectra of Polyatomic Molecules (Beijing: Science Press) pp291---301 (in Chinese) [赫兹堡G著 (王鼎昌译) 1986分子光谱与分子结构 (第二卷) 多原子分子的红外光谱与拉曼光谱 (北京:科学出版社)第291--301页]
[10] Wu Y Q, Jiang G C, You J L, Hou H Y, Chen H 2002 J. At. Mol. Phys. 19 433 (in Chinese) [吴永全, 蒋国昌, 尤静林, 侯怀宇, 陈辉 2002 原子与分子 19 433]
[11] Duan R G, Liang K M, Gu S R 1998 J. Inorg. Mater. 13 593 (in Chinese) [段仁官, 梁开明, 顾守仁 1998 无机材料学报 13 593]
[12] de Maeyer E A, Verbeeck R M, Vercruysse C W 2002 Dent. Res. 81 552
[13] Iguchi Y, Kashio S, Goto T, Nishina Y, Fuwa T 1981 Can. Metall. Quart. 20 51
[14] McMillan P 1984 Am. Mineral. 69 622
[15] You J L, Jiang G C, Hou H Y, Hou H Y, Chen H, Wu Y Q, Xu K D 2004 J. Raman Spectrosc. 36 237
[16] Dowty E 1987 Phys. Chem. Miner. 14 80
[17] Hu N, Yu H, Zhang M, Zhang P, Wang Y Z, Zhao L J 2011 Phys. Chem. Chem. Phys. 13 1499
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[1] Wang Y, Ohwaki J 1993 Appl. Phys. Lett. 63 3268
[2] Tikhomirov V K, Driesen K, Görller-Walrand C, Mortier M 2007 Opt. Express 15 9535
[3] Meng J, Zhao L J, Yu H, Tang L Q, Liang Q, Yu X Y, Tang B Q, Su J, Xu J J 2005 Acta Phys. Sin. 54 1442 (in Chinese) [孟婕, 赵丽娟, 余华, 唐莉勤, 梁沁, 禹宣伊, 唐伯权, 苏静, 许京军 2005 54 1442]
[4] Chen D Q, Wang Y S, Yu Y L, Ma E, Liu F 2007 J. Phys. Chem. Solids 68 193
[5] Mysen B O, Virgo D, Kushiro I 1981 Am. Mineral. 66 678
[6] Hatta B, Tomozawa M 2008 J. Non-Cryst. Solids 354 3184
[7] Song S X, Chen J S, Zhen W H, Deng W 2009 Glass Enamel 37 5 (in Chinese) [宋树欣, 程金树, 郑伟宏, 邓炜 2009 玻璃与搪瓷 37 5]
[8] Gan F X 1992 Optical and Spectroscopic Properties of Glass (Shanghai: Shanghai Scientific and Technical Publishers) pp39--54 (in Chinese) [干福熹 1992 玻璃的光学和光谱性质(上海:上海科学技术出版社) 第39---54页]
[9] Herzberg G (translated by Wang D C) 1986 Molecular Spectra and Molecular Structure II Infrared and Raman Spectra of Polyatomic Molecules (Beijing: Science Press) pp291---301 (in Chinese) [赫兹堡G著 (王鼎昌译) 1986分子光谱与分子结构 (第二卷) 多原子分子的红外光谱与拉曼光谱 (北京:科学出版社)第291--301页]
[10] Wu Y Q, Jiang G C, You J L, Hou H Y, Chen H 2002 J. At. Mol. Phys. 19 433 (in Chinese) [吴永全, 蒋国昌, 尤静林, 侯怀宇, 陈辉 2002 原子与分子 19 433]
[11] Duan R G, Liang K M, Gu S R 1998 J. Inorg. Mater. 13 593 (in Chinese) [段仁官, 梁开明, 顾守仁 1998 无机材料学报 13 593]
[12] de Maeyer E A, Verbeeck R M, Vercruysse C W 2002 Dent. Res. 81 552
[13] Iguchi Y, Kashio S, Goto T, Nishina Y, Fuwa T 1981 Can. Metall. Quart. 20 51
[14] McMillan P 1984 Am. Mineral. 69 622
[15] You J L, Jiang G C, Hou H Y, Hou H Y, Chen H, Wu Y Q, Xu K D 2004 J. Raman Spectrosc. 36 237
[16] Dowty E 1987 Phys. Chem. Miner. 14 80
[17] Hu N, Yu H, Zhang M, Zhang P, Wang Y Z, Zhao L J 2011 Phys. Chem. Chem. Phys. 13 1499
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