Reduction of CO<sub>2</sub> by TiO<sub>2</sub> nanoparticles through friction in water

Li Peng-Cheng; Tang Chong-Yang; Cheng Liang; Hu Yong-Ming; Xiao Xiang-Heng; Chen Wan-Ping

doi:10.7498/aps.70.20210210

Abstract

The friction between some nanomaterials and teflon magnetic stirring rods has recently been found responsible for dye degradation by magnetic stirring in dark. In this work, a study is conducted on the reduction of CO₂ by TiO₂ nanoparticles under magnetic stirring in water. In a 100-mL reactor filled with 50-mL water, 1.00-g TiO₂ nanoparticles and 1-atm CO₂, 50-h magnetic stirring results in the formation of 6.65 × 10^–6 (volume fraction) CO, 2.39 × 10^–6 CH₄ and 0.69 × 10^–6 H₂; while in a reactor without TiO₂ nanoparticles, the same magnetic stirring leads only 2.22 × 10^–6 CO and 0.98 × 10^–6 CH₄ to form. Four magnetic stirring rods are used simultaneously to further enhance the stirring, and 50-h magnetic stirring can form 19.94 × 10^–6 CO, 2.33 × 10^–6 CH₄, and 2.06 × 10^–6 H₂. A mechanism for the catalytic role of TiO₂ nanoparticles in the reduction of CO₂ and H₂O is established, which is based on the excitation of electron-hole pairs in TiO₂ by mechanical energy absorbed through friction. This finding clearly demonstrates that nanostructured semiconductors are able to utilize mechanical energy obtained through friction to reduce CO₂, thus providing a new direction for developing and utilizing the mechanical energy harvested from ambient environment.

Keywords:

Authors and contacts

1.
School of Physics and Technology, Wuhan University, Wuhan 430072, China
2.
School of Physics and Electronic Science, Hubei University, Wuhan 430062, China

Corresponding author: Chen Wan-Ping, wpchen@whu.edu.cn

Funds: Project supported by the National Natural Science Foundation of China (Grant No. U2067207) and the National Key R&D Program of China (Grant No. 2020YFB2008800).

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References

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Cited By

图 1 二氧化钛纳米颗粒的SEM照片

Figure 1. An SEM micrograph taken for as-received TiO₂ nanoparticles.

DownLoad: Full-Size Img PowerPoint

图 2 单个磁力搅拌棒分别搅拌50 h溶解有CO₂的水及溶解有CO₂并分散有TiO₂纳米粉的水所产生的气体产物

Figure 2. Gases produced from water dissolved with CO₂ through 50 h magnetic stirring using a PTFE (poly tetra fluoroethylene) magnetic stirring rod. There were no TiO₂ nanoparticles in water in the reference test.

DownLoad: Full-Size Img PowerPoint

图 3 分别经过50, 100, 150 h磁力搅拌的气体产物, 在磁力搅拌中同时采用4个特氟龙磁力搅拌棒

Figure 3. Gases produced from water dissolved with CO₂ through 50, 100 and 150 h, separately, magnetic stirring using four PTFE magnetic stirring rods.

DownLoad: Full-Size Img PowerPoint

图 4 生成的气体体积分数与磁力搅拌时间的关系: 对溶解有CO₂并分散有TiO₂纳米粉的50 mL的水采用4个特氟龙磁力搅拌棒进行搅拌

Figure 4. Stirring time dependence of CO, CH₄ and H₂ produced from water dissolved with CO₂ and dispersed with TiO₂ nanoparticles through magnetic stirring using four PTFE magnetic stirring rods.

DownLoad: Full-Size Img PowerPoint

图 5 对含有TiO₂纳米粉的苯二甲酸钠溶液在室温及黑暗条件下用4个搅拌棒磁力搅拌后的荧光光谱(激发波长为315 nm)

Figure 5. Fluorescence spectra (excitation wavelength: 315 nm) of sodium terephthalate solution containing TiO₂ nanoparticles after being magnetically stirred using four stirring rods at room temperature in dark.

DownLoad: Full-Size Img PowerPoint

图 6 TiO₂纳米颗粒摩擦催化还原CO₂和水的示意图

Figure 6. Schematic illustration of the tribocatalytic reduction of CO₂ and H₂O by TiO₂ nanoparticles under magnetic stirring.

DownLoad: Full-Size Img PowerPoint

map

[1]	李冬冬, 王丽莉 2012 61 034212 Google Scholar Li D D, Wang L L 2012 Acta Phys. Sin. 61 034212 Google Scholar
[2]	李平, 李海金, 涂文广, 周勇, 邹志刚 2015 64 094209 Google Scholar Li P, Li H J, Tu W G, Zhou Y, Zou Z G 2015 Acta Phys. Sin. 64 094209 Google Scholar
[3]	吴化平, 令欢, 张征, 李研彪, 梁利华, 柴国钟 2017 66 167702 Google Scholar Wu H P, Ling H, Zhang Z, Li Y B, Liang L H, Chai G Z 2017 Acta Phys. Sin. 66 167702 Google Scholar
[4]	赵娟, 胡慧芳, 曾亚萍, 程彩萍 2013 62 158104 Google Scholar Zhao J, Hu H F, Zeng Y P, Cheng C P 2013 Acta Phys. Sin. 62 158104 Google Scholar
[5]	崔宗杨, 谢忠帅, 汪尧进, 袁国亮, 刘俊明 2020 69 127706 Google Scholar Cui Z Y, Xie Z S, Wang Y J, Yuan G L, Liu J M 2020 Acta Phys. Sin. 69 127706 Google Scholar
[6]	Ran J, Jaroniec M, Qiao S Z 2018 Adv. Mater. 30 1704649 Google Scholar
[7]	Kreft S, Wei D, Junge H, Beller M 2020 Energy Chem. 2 100044 Google Scholar
[8]	Wang X, Li Z, Yang X 2015 J. Mol. Sci. 31 190201
[9]	吴晔盛, 刘启, 曹杰, 李凯, 程广贵, 张忠强, 丁建宁, 蒋诗宇 2019 68 190201 Google Scholar Wu Y S, Liu Q, Cao J, Li K, Cheng G G, Zhang Z Q, Ding J N, Jiang S Y 2019 Acta Phys. Sin. 68 190201 Google Scholar
[10]	韩杰敏, 王梅, 仝召民, 马一飞 2019 无机材料学报 34 839 Google Scholar Han J M, Wang M, Tong Z M, Ma Y F 2019 J. Inorg. Mater. 34 839 Google Scholar
[11]	程广贵, 张伟, 方俊, 蒋诗宇, 丁建宁, Pesika N S, 张忠强, 郭立强, 王莹 2016 65 060201 Google Scholar Cheng G G, Zhang W, Fang J, Jiang S Y, Ding J N, Pesika N S, Zhang Z Q, Guo L Q, Wang Y 2016 Acta Phys. Sin. 65 060201 Google Scholar
[12]	秦杰明, 田立飞, 赵东旭, 蒋大勇, 曹建明, 丁梦, 郭振 2011 60 107307 Google Scholar Qin J M, Tian L F, Zhao D X, Jiang D Y, Cao J M, Ding M, Guo Z 2011 Acta Phys. Sin. 60 107307 Google Scholar
[13]	Deng J N, Kuang X, Liu R Y, Ding W B, Wang A C, Lai Y C, Dong K, Wen Z, Wang Y X, Wang L L, Qi H J, Zhang T, Wang Z L 2018 Adv. Mater. 30 1705918 Google Scholar
[14]	Wu J M, Chang W E, Chang Y T, Chang C K 2016 Adv. Mater. 28 3718 Google Scholar
[15]	Liang Z, Yan C F, Rtimi S, Bandara J 2019 Appl. Catal. B-Environ 241 256 Google Scholar
[16]	洪元婷, 马江平, 武峥, 应静诗, 尤慧琳, 贾艳敏 2018 67 107702 Google Scholar Hong Y T, Ma J P, Wu Z, Ying J S, You H L, Jia Y M 2018 Acta Phys. Sin. 67 107702 Google Scholar
[17]	徐姝雅, 刘治宏, 张淮, 于金冉 2019 化学学报 77 427 Xu S Y, Liu Z H, Zhang H, Yu J R 2019 Acta Phys. Sin. 77 427
[18]	Starr M B, Shi J, Wang X D 2012 Angew. Chem. Int. Ed. 51 5962 Google Scholar
[19]	You H, Wu Z, Zhang L, Ying Y, Liu Y, Fei L, Chen X, Jia Y, Wang Y, Wang F, Ju S, Qiao J, Lam C H, Huang H 2019 Angew. Chem. 58 11779 Google Scholar
[20]	Feng W, Yuan J, Zhang L, Hu W, Wu Z, Wang X, Huang X, Liu P, Zhang S 2020 Appl. Catal. B-Environ 277 119250 Google Scholar
[21]	Su R, Hsain H A, Wu M, Zhang D, Hu X, Wang Z, Wang X, Li F T, Chen X, Zhu L, Yang Y, Yang Y, Lou X, Pennycook S J 2019 Angew. Chem. 131 15220 Google Scholar
[22]	Yein W T, Wang Q, Liu Y, Li Y, Jian J H, Wu X H 2020 J. Environ. Chem. Eng. 8 103626 Google Scholar
[23]	Kang Z H, Qin N, Lin E Z, Wu J, Yuan B W, Bao D H 2020 J. Cleaner Prod. 261 121125 Google Scholar
[24]	Hao A, Ning X, Cao Y, Xie J, Jia D 2020 Mater. Chem. Front. 4 2096 Google Scholar
[25]	Wei Y, Zhang Y, Geng W, Su H, Long M 2019 Appl. Catal. B-Environ 259 118084 Google Scholar
[26]	Ismail M, Wu Z, Zhang L, Ma J, Jia Y, Hu Y, Wang Y 2019 Chemosphere 228 212 Google Scholar
[27]	Lin J H, Tsao Y H, Wu M H, Chou T M, Lin Z H, Wu J M 2017 Nano Energy 31 575 Google Scholar
[28]	Feng Y, Ling L, Wang Y, Xu Z, Cao F, Li H, Bian Z 2017 Nano Energy 40 481 Google Scholar
[29]	Zhu R, Xu Y, Bai Q, Wang Z, Guo X, Kimura H 2018 Chem. Phys. Lett. 702 26 Google Scholar
[30]	Nie Q, Xie Y, Ma J, Wang J, Zhang G 2020 J. Cleaner Prod. 242 118532 Google Scholar
[31]	Liu D, Song Y, Xin Z, Liu G, Jin C, Shan F 2019 Nano Energy 65 104024 Google Scholar
[32]	Li P, Wu J, Wu Z, Jia Y, Ma J, Chen W, Zhang L, Yang J, Liu Y 2019 Nano Energy 63 103832 Google Scholar
[33]	Lei H, Wu M, Mo F, Ji S, Dong X, Wu Z, Gao J, Yang Y, Jia Y 2020 Nano Energy 78 105290 Google Scholar
[34]	Zhao J, Chen L, Luo W, Li H, Wu Z, Xu Z, Zhang Y, Zhang H, Yuan G, Gao J, Jia Y 2020 Ceram. Int. 46 25293 Google Scholar
[35]	Yang B, Chen H, Guo X, Wang L, Xu T, Bian J, Yang Y, Liu Q, Du Y, Lou X 2020 J. Mater. Chem. C 8 14845 Google Scholar
[36]	Wu M, Lei H, Chen J, Dong X 2020 J. Colloid Interface Sci. 587 883
[37]	Ishibashi K I, Fujishima A, Watanabe T, Hashimoto K 2000 Electrochem. Commun. 2 207 Google Scholar
[38]	Baytekin B, Baytekin H T, Grzybowski B A 2012 J. Am. Chem. Soc. 134 7223 Google Scholar
[39]	Heinicke G, Hennig H P, Linke E, Steinike U, Thiessen K P, Meyer K 1984 Cryst. Res. Technol. 19 1424 Google Scholar
[40]	Kajdas C, Hiratsuka K 2009 Proc. Inst. Mech. Eng., Part J 223 827 Google Scholar
[41]	Park J Y, Salmeron M 2014 Chem. Rev. 114 677 Google Scholar
[42]	Manini N, Mistura G, Paolicelli G, Tosatti E, Vanossi A 2017 Adv. Phys.: X 2 569
[43]	Qi Y, Park J Y, Hendriksen B L M, Ogletree D F, Salmeron M 2008 Phys. Rev. B 77 184105 Google Scholar
[44]	Schneider J, Matsuoka M, Takeuchi M, Zhang J, Horiuchi Y, Anpo M, Bahnemann D W 2014 Chem. Rev. 114 9919 Google Scholar
[45]	Fujishima A, Zhang X, Tryk D 2008 Surf. Sci. Rep. 63 515 Google Scholar
[46]	Al-Mamoori A, Krishnamurthy A, Rownaghi A A, Rezaei F 2017 Energy Technol. 5 834 Google Scholar

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Reduction of CO₂ by TiO₂ nanoparticles through friction in water

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Corresponding author: Chen Wan-Ping, wpchen@whu.edu.cn

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Reduction of CO2 by TiO2 nanoparticles through friction in water

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Corresponding author: Chen Wan-Ping, wpchen@whu.edu.cn

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Reduction of CO₂ by TiO₂ nanoparticles through friction in water