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Using trans-2-butene and hydrogen as the precursor, the glow discharge polymer (GDP) films are successfully coated on glass microspheres with diameters of 350—400 μm and thicknesses of 2.5—3 μm by the glow discharge polymerization technology. Glass/GDP microsphere is heated to test its thermal stability, whose process is the same as the D2 gas charge procedure. The chemical structures, the thermal stabilities of the GDP films, the morphologies of glass/GDP microspheres are characterized by the FT-IR, TG, stereoscopic microscope and X-radiography technology. The Results show that the C/H and C C in GDP films decrease as pressure increases. Their thermal stabilities are better, and the adhesion between GDP film and glass microsphere is enhanced when the GDP coatings are fabricated at lower pressures.
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Keywords:
- glass microspheres /
- glow discharge polymer films /
- thermal stability /
- adhesion
[1] Zhang Q, Yoon S F, Rusli, Yang H, Ahn J 1998 J.Apply.Phys. 83 1349
[2] Chen K C, Cook R C, Huang H, Letts S A, Nikroo A 2006 Fusion Science and Technology 49 750
[3] Haan S W, Herrmann M C, Dittrich T R, Fetterman A J, Marinak M M, Munro D H, Pollaine S M, Salmonson J D, Strobel G L, Suter L J 2005 Phys. Plasmas 12 056316
[4] Ju J H, Xia Y B, Zhang W L, Wang L J, Shi W M, Huang Z M, Li Z F, Zheng G Z, Tang D Y 2000 Acta Phys. Sin. 49 2311 (in Chinese) [居建华﹑夏义本﹑张伟丽、王林军﹑史为民﹑黄志明﹑李志锋﹑郑国珍﹑汤定元 2000 49 2311]
[5] Letts S A, Meyers D W, Witt L A 1981 J. Vac. Sci. Technol. 19 739
[6] Zhang Z W,Li B,Tang Y J,Lei H L 2007 High Power Laser and Particle Beams 10 1664(in Chinese)[张占文、李 波、唐永建、雷海乐 2007 强激光与离子束 10 1664]
[7] Zhang B L, He Z B, Wu W D, Liu X H, Yang X D 2009 Acta Phys. Sin. 58 6436(in Chinese)[张宝玲、何智兵、吴卫东、刘兴华、杨向东2009 58 6436]
[8] Qiu L H,Wei Y,Tang Y J,Fu Y B,Zheng Y M,Shi T 2001 Atomic Energy Science and Technolgy 1 60(in Chinese)[邱会龙、魏芸、唐永建、傅依备、郑永铭、师 韬 2001 原子能科学技术 1 60]
[9] Ristein J, Stief R T, Ley L 1998 Journal of Applied Physics 84 3836
[10] Kim M H, Lee J Y 1991 Journal of Materials Science 26 4787
[11] Bounouh Y, Theye M L, Dehbi-Alaoui A, Matthews A, Stoquert J P 1995 Physical Review B 51 9597
[12] Qing Zhang, Yoon S F, Rusli, Yang H, Ahn J 1998 J. Appl. Phys. 83 1349
[13] Czechowicz D G, Castillo E R, Nikroo A 2002 General Atomics Report GA-A23753
[14] Nikroo A, Czechowicz D G, Castillo E R, Pontelandolfo J M 2002 General Atomics Report GA-A23758
[15] Tersoff T 1991 Phys. Revs. B 44 12039
[16] Robertson J 2002 Materials Science and Engineering R 37 129
[17] Tomasella E, Meunierb C, Mikhailov S 2001 Surface and Coatings Technology 141 286
[18] Zhang B L, He Z B, Wu W D, Yang X D, Liu X H 2009 Atomic Energy Science and Technolgy 43 776(in Chinese)[张宝玲、何智兵、吴卫东、杨向东、刘兴华 2009 原子能科学技术 43 776]
[19] Yang H N, Tweet D J, Ma Y J, Ngnyen T 1998 Appl.Phys.Lett. 73 1514
[20] Jiang L, Shen L, Zhen Q 2004 Journal of Functional Materials 35 142(in Chinese) [江 磊、沈 烈、郑 强 2004 功能材料 35 142]
[21] Chen W L, Gu P F, Wang Y, Zhang Y G, Liu X 2008 Acta Phys. Sin. 57 4316 (in Chinese)[陈为兰、顾培夫、王 颖、章岳光、刘 旭2008 57 4316]
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[1] Zhang Q, Yoon S F, Rusli, Yang H, Ahn J 1998 J.Apply.Phys. 83 1349
[2] Chen K C, Cook R C, Huang H, Letts S A, Nikroo A 2006 Fusion Science and Technology 49 750
[3] Haan S W, Herrmann M C, Dittrich T R, Fetterman A J, Marinak M M, Munro D H, Pollaine S M, Salmonson J D, Strobel G L, Suter L J 2005 Phys. Plasmas 12 056316
[4] Ju J H, Xia Y B, Zhang W L, Wang L J, Shi W M, Huang Z M, Li Z F, Zheng G Z, Tang D Y 2000 Acta Phys. Sin. 49 2311 (in Chinese) [居建华﹑夏义本﹑张伟丽、王林军﹑史为民﹑黄志明﹑李志锋﹑郑国珍﹑汤定元 2000 49 2311]
[5] Letts S A, Meyers D W, Witt L A 1981 J. Vac. Sci. Technol. 19 739
[6] Zhang Z W,Li B,Tang Y J,Lei H L 2007 High Power Laser and Particle Beams 10 1664(in Chinese)[张占文、李 波、唐永建、雷海乐 2007 强激光与离子束 10 1664]
[7] Zhang B L, He Z B, Wu W D, Liu X H, Yang X D 2009 Acta Phys. Sin. 58 6436(in Chinese)[张宝玲、何智兵、吴卫东、刘兴华、杨向东2009 58 6436]
[8] Qiu L H,Wei Y,Tang Y J,Fu Y B,Zheng Y M,Shi T 2001 Atomic Energy Science and Technolgy 1 60(in Chinese)[邱会龙、魏芸、唐永建、傅依备、郑永铭、师 韬 2001 原子能科学技术 1 60]
[9] Ristein J, Stief R T, Ley L 1998 Journal of Applied Physics 84 3836
[10] Kim M H, Lee J Y 1991 Journal of Materials Science 26 4787
[11] Bounouh Y, Theye M L, Dehbi-Alaoui A, Matthews A, Stoquert J P 1995 Physical Review B 51 9597
[12] Qing Zhang, Yoon S F, Rusli, Yang H, Ahn J 1998 J. Appl. Phys. 83 1349
[13] Czechowicz D G, Castillo E R, Nikroo A 2002 General Atomics Report GA-A23753
[14] Nikroo A, Czechowicz D G, Castillo E R, Pontelandolfo J M 2002 General Atomics Report GA-A23758
[15] Tersoff T 1991 Phys. Revs. B 44 12039
[16] Robertson J 2002 Materials Science and Engineering R 37 129
[17] Tomasella E, Meunierb C, Mikhailov S 2001 Surface and Coatings Technology 141 286
[18] Zhang B L, He Z B, Wu W D, Yang X D, Liu X H 2009 Atomic Energy Science and Technolgy 43 776(in Chinese)[张宝玲、何智兵、吴卫东、杨向东、刘兴华 2009 原子能科学技术 43 776]
[19] Yang H N, Tweet D J, Ma Y J, Ngnyen T 1998 Appl.Phys.Lett. 73 1514
[20] Jiang L, Shen L, Zhen Q 2004 Journal of Functional Materials 35 142(in Chinese) [江 磊、沈 烈、郑 强 2004 功能材料 35 142]
[21] Chen W L, Gu P F, Wang Y, Zhang Y G, Liu X 2008 Acta Phys. Sin. 57 4316 (in Chinese)[陈为兰、顾培夫、王 颖、章岳光、刘 旭2008 57 4316]
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