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AlSb/GaAs(001)失配位错的高分辨电子显微学研究

温才 李方华 邹进 陈弘

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AlSb/GaAs(001)失配位错的高分辨电子显微学研究

温才, 李方华, 邹进, 陈弘

High-resolution electron microscopy of misfit dislocations in AlSb/GaAs(001) system

Wen Cai, Li Fang-Hua, Zou Jin, Chen Hong
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  • 用200 kV 六硼化镧光源的高分辨透射电子显微镜观察了AlSb/GaAs(001)外延薄膜的失配位错,结合解卷处理方法把[110]高分辨电子显微像转换为试样的结构投影图,其分辨率接近电子显微镜的信息极限.根据赝弱相位物体近似像衬理论,通过分析AlSb薄膜完整区解卷像的衬度随试样厚度的变化,确定了哑铃原子对中Al和Sb原子的位置.在此基础上构建出失配位错的结构模型,再结合模拟像与实验像的匹配,确定了AlAs型界面以及Lomer和60°两类失配全位错的核心结构.
    The detailed core structures of misfit dislocations in the AlSb/GaAs(001) heterostructure system were studied by 200 kV LaB6 filament high-resolution electron microscope. In combination with image deconvolution, the[110] images were transformed into the projected structure maps, and the image resolution was enhanced up to the information limit of the microscope. To distinguish Al and Sb atoms in the AlSb film, the image contrast change with the sample thickness was analyzed for the perfect region in deconvoluted image, and the positions of Al and Sb atoms in the dumbbells were determined based on the image contrast theory of the pseudo-weak-phase object approximation. Then the structure models of two types of misfit dislocations were constructed. As the simulated images are in good agreement with the experimental images, the AlAs type interface and the core structures of obtained Lomer and 60° misfit dislocations were determined.
    • 基金项目: 国家自然科学基金(批准号:50672124)资助的课题.
    [1]

    [1]Kroemer H 2004 Physica E 20 196

    [2]

    [2]Subbanna S, Gaines J, Tuttle G, Kroemer H, Chalmers S, English J H 1989 J. Vac. Sci. Technol. B 7 289

    [3]

    [3]Kim H S, Noh Y K, Kim M D, Kwon Y J, Oh J E, Kim Y H, Lee J Y, Kim S G, Chung K S 2007 J. Cryst. Growth 301-302 230[4]Lomer W M 1951 Philos. Mag. 42 1327

    [4]

    [5]Marshall A F, Aubertine D B, Nix W D, McIntyre P C 2005 J. Mater. Res. 20 447

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    [6]Tillmann K, Houben L, Thust A 2006 Philos. Mag. 86 4589

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    [7]Qian W, Skowronski M, Kaspi R, de Graef M, Dravid V P 1997 J. Appl. Phys. 81 7268

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    [8]Jallipalli A, Balakrishnan G, Huang S H, Khoshakhlagh A, Dawson L R, Huffaker D L 2007 J. Cryst. Growth 303 449

    [8]

    [9]Trampert A, Tournie E, Ploog K H 1995 Appl. Phys. Lett. 66 2265

    [9]

    ]Chen F R, Kai J J, Chang L, Wang J Y, Chen W J 1999 J. Electron Microsc. 48 827

    [10]

    ]He W Z, Li F H, Chen H, Kawasaki K, Oikawa T 1997 Ultramicroscopy 70 1

    [11]

    ]Wang D, Zou J, He W Z, Chen H, Li F H, Kawasaki K, Oikawa T 2004 Ultramicroscopy 98 259

    [12]

    ]Wang D, Chen H, Li F H, Kawasaki K, Oikawa T 2002 Ultramicroscopy 93 139

    [13]

    ]Scherzer O 1949 J. Appl. Phys. 20 20

    [14]

    ]Han F S, Fan H F, Li F H 1986 Acta Crystallogr. A 42 353

    [15]

    ]Hu J J, Li F H 1991 Ultramicroscopy 35 339

    [16]

    ]Li F H, Wang D, He W Z, Jiang H 2000 J. Electron Microsc. 49 17

    [17]

    ]Tang C Y, Li F H, Wang R, Zou J, Zheng X H, Liang J W 2007 Phys. Rev. B 75 184103

    [18]

    ]Li F H, Tang D 1985 Acta Crystallogr. A 41 376

    [19]

    ]Thon F 1966 Z. Naturforsch. 210 476

    [20]

    ]Hornstra J 1958 J. Phys. Chem. Solids 5 129

    [21]

    ]Vila A, Cornet A, Morante J R, Ruterana P, Loubradou M, Bonnet R, Gonzalez Y, Gonzalez L 1995 Philos. Mag. A 71 85

    [22]

    ]Lopatin S, Pennycook S J, Narayan J, Duscher G 2002 Appl. Phys. Lett. 81 2728

    [23]

    ]Hull D, Bacon D J 2001 Introduction to Dislocations (Oxford: Butterworth-Heinemann) p123[25]Zou J, Cockayne D J H 1993 J. Appl. Phys. 74 925

    [24]

    ]Zou J, Cockayne D J H 1993 Appl. Phys. Lett. 63 2222

    [25]

    ]Cowley J M, Moodie A F 1957 Acta Crystallogr. 10 609

  • [1]

    [1]Kroemer H 2004 Physica E 20 196

    [2]

    [2]Subbanna S, Gaines J, Tuttle G, Kroemer H, Chalmers S, English J H 1989 J. Vac. Sci. Technol. B 7 289

    [3]

    [3]Kim H S, Noh Y K, Kim M D, Kwon Y J, Oh J E, Kim Y H, Lee J Y, Kim S G, Chung K S 2007 J. Cryst. Growth 301-302 230[4]Lomer W M 1951 Philos. Mag. 42 1327

    [4]

    [5]Marshall A F, Aubertine D B, Nix W D, McIntyre P C 2005 J. Mater. Res. 20 447

    [5]

    [6]Tillmann K, Houben L, Thust A 2006 Philos. Mag. 86 4589

    [6]

    [7]Qian W, Skowronski M, Kaspi R, de Graef M, Dravid V P 1997 J. Appl. Phys. 81 7268

    [7]

    [8]Jallipalli A, Balakrishnan G, Huang S H, Khoshakhlagh A, Dawson L R, Huffaker D L 2007 J. Cryst. Growth 303 449

    [8]

    [9]Trampert A, Tournie E, Ploog K H 1995 Appl. Phys. Lett. 66 2265

    [9]

    ]Chen F R, Kai J J, Chang L, Wang J Y, Chen W J 1999 J. Electron Microsc. 48 827

    [10]

    ]He W Z, Li F H, Chen H, Kawasaki K, Oikawa T 1997 Ultramicroscopy 70 1

    [11]

    ]Wang D, Zou J, He W Z, Chen H, Li F H, Kawasaki K, Oikawa T 2004 Ultramicroscopy 98 259

    [12]

    ]Wang D, Chen H, Li F H, Kawasaki K, Oikawa T 2002 Ultramicroscopy 93 139

    [13]

    ]Scherzer O 1949 J. Appl. Phys. 20 20

    [14]

    ]Han F S, Fan H F, Li F H 1986 Acta Crystallogr. A 42 353

    [15]

    ]Hu J J, Li F H 1991 Ultramicroscopy 35 339

    [16]

    ]Li F H, Wang D, He W Z, Jiang H 2000 J. Electron Microsc. 49 17

    [17]

    ]Tang C Y, Li F H, Wang R, Zou J, Zheng X H, Liang J W 2007 Phys. Rev. B 75 184103

    [18]

    ]Li F H, Tang D 1985 Acta Crystallogr. A 41 376

    [19]

    ]Thon F 1966 Z. Naturforsch. 210 476

    [20]

    ]Hornstra J 1958 J. Phys. Chem. Solids 5 129

    [21]

    ]Vila A, Cornet A, Morante J R, Ruterana P, Loubradou M, Bonnet R, Gonzalez Y, Gonzalez L 1995 Philos. Mag. A 71 85

    [22]

    ]Lopatin S, Pennycook S J, Narayan J, Duscher G 2002 Appl. Phys. Lett. 81 2728

    [23]

    ]Hull D, Bacon D J 2001 Introduction to Dislocations (Oxford: Butterworth-Heinemann) p123[25]Zou J, Cockayne D J H 1993 J. Appl. Phys. 74 925

    [24]

    ]Zou J, Cockayne D J H 1993 Appl. Phys. Lett. 63 2222

    [25]

    ]Cowley J M, Moodie A F 1957 Acta Crystallogr. 10 609

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出版历程
  • 收稿日期:  2009-12-21
  • 修回日期:  2009-12-29
  • 刊出日期:  2010-03-15

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