中能高浓度氦离子注入对钨微观结构的影响

郭洪燕; 夏敏; 燕青芝; 郭立平; 陈济红; 葛昌纯

doi:10.7498/aps.65.077803

摘要

采用15 keV, 剂量11017/cm2, 温度为600 ℃氦离子注入钨, 分别以块体钨研究氦离子对钨的表面损伤; 以超薄的钨透射电镜样品直接注入氦离子, 研究该条件下钨的微观结构变化, 以了解氦离子与钨的相互作用过程; 采用扫描电子显微镜、聚焦离子束扫描显微镜、透射电子显微镜、高分辨透射电子显微镜等分析手段研究氦离子注入对钨表面显微结构的影响及氦泡在钨微观结构演化中的作用.

关键词:

Bulk tungsten and tungsten transmission electron microscopy (TEM) lamella are implanted with 15 keV helium ions at about 873 K to study the microstructure evolution. The samples are implanted to about 11017 He+/cm2. The projected range of the helium ion in tungsten is about 43.9 nm, calculated with the stopping and range of ions in matter program (the SRIM code). The density of pores with diameters ranging from 90 nm to 430 nm is detected on the surface of helium implanted bulk tungsten by field emission scanning electron microscopy. Blistering is also observed on the surface of helium implanted bulk tungsten. The TEM results indicate that fuzz microstructure is formed in helium implanted tungsten TEM lamella, and stacking faults and micro-pores are observed in the fuzz structure. Besides, the density of nano-scaled helium bubbles is detected around the mirco-pores.

Keywords:

tungsten /
medium energy and high density He+ implanted /
helium bubbles /
microstructures

作者及机构信息

1.
中国矿业大学(北京), 深部岩土力学与地下工程国家重点实验室, 北京 100083;

2.
北京科技大学材料科学与工程学院, 特种陶瓷粉末冶金研究所, 北京 10083;

3.
武汉大学物理科学与技术学院加速器实验室, 武汉 430072

通信作者: 夏敏, xmdsg@ustb.edu.cn;ccge@mater.ustb.edu.cn ; 葛昌纯, xmdsg@ustb.edu.cn;ccge@mater.ustb.edu.cn

基金项目: 国家重点基础研究发展计划 (批准号: 2010GB109000, 2014GB123000)资助的课题.

Authors and contacts

1.
State Key Laboratory for Geomechanics and Deep Underground Engineering, China University of Mining and Technology, Beijing 100083, China;

2.
Institute of Special Ceramics and Powder Metallurgy, School of Materials Science and Engineering, University of Science and Technology Beijing, Beijing 100083, China;

3.
Accelerator Laboratory, School of Physics and Technology, Wuhan University, Wuhan 430072, China

Corresponding author: Xia Min, xmdsg@ustb.edu.cn;ccge@mater.ustb.edu.cn ; Ge Chang-Chun, xmdsg@ustb.edu.cn;ccge@mater.ustb.edu.cn

Funds: Project supported by the National Basic Research Program of China (Grant Nos. 2010GB109000, 2014GB123000).

参考文献

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[2]	Xia M, Yan Q Z, Xu L, Guo H Y, Zhu L X, Ge C C 2013 J. Nucl. Mater. 434 85
[3]	Xia M, Yan Q Z, Xu L, Zhu L X, Guo H Y, Ge C C 2013 J. Nucl. Mater. 430 216
[4]	Andreani R, Diegele E, Laesser R, van der Schaaf B 2004 J. Nucl. Mater. 329-333 20
[5]	Morenzo B, Edgar B, Karin B, Luigi D P, Robin F, Luciano G, Stephan H, Claudio N, Prachai N, Aldo P, Neill T, David W 2005 Fusion Eng. Des. 75-79 1173
[6]	Maisonnier D, Cook I, Pierre S, Lorenzo B, Luigi D P, Luciano G, Prachai N, Aldo P 2006 Fusion Eng. Des. 81 1123
[7]	Lässer R, Baluc N, Boutard J L, Diegele E, Dudarev S, Gasparotto M, Möslang A, Pippan B, Riccardi B, van der Schaaf B 2007 Fusion Eng. Des. 82 511
[8]	Linke J, Akiba M, Bolt H, Breitbach G, Duwe R, Makhankov A, Ovchinnikov I, Rödig M, Wallura E 1997 J. Nucl. Mater. 241-243 1210
[9]	Singheiser L, Hirai T, Linke J, Pintsuk M, Rödig M 2009 Trans. Indian Inst. Metals. 62 123
[10]	Philipps V 2011 J. Nucl. Mater. 415 S2
[11]	Song B, Guo L P, Li M, Li C J, Ye M S, Fu D J, Fan X J 2007 Nuclear Techniques 30 777 (in Chinese) [宋搏, 郭立平, 黎明, 李传佳, 叶明生, 付德军, 范湘军 2007 核技术 30 777]
[12]	Yu J N, Sha J J, Yu G 2013 Proceedings of the 16th International Conference on Fusion Reactor Materials (ICFRM-16) Beijing, China, October 20-26, 2013
[13]	Ziegler J F, Biersack J P, Littmark U 1985 Ion Implantation Science and Technology (New York: Academic Press) p51
[14]	Wang T Q, Shen Y P, Zhang R Q, Wang S W, Zhang S F 2000 High Power Laser and Particle Beams 12 339 (in Chinese) [王同权, 沈永平, 张若棋, 王尚武, 张树发 2000 强激光与粒子束 12 339]
[15]	Wang P X, Song J S 2002 Material of Helium and Tritium Permeation (Beijing: National Defence Industry Press) p30 (in Chinese) [王佩璇, 宋家树 2002 材料中的氦及氚渗透(北京: 国防工业出版社) 第30页]
[16]	Hartley F R 1973 The Chemistry of Platinum and Palladium: with Particular Reference to Complexes of the Elements (London:Applied Science Publishers) p5334
[17]	Kajita S, Sakaguchi W, Ohno N, Yoshida N, Saeki T 2009 Nucl. Fusion 49 95005
[18]	Cipiti B B, Kulcinski G L 2005 J. Nucl. Mater. 347 298
[19]	Kajita S, Yoshida N, Yoshihara R, Ohno N, Yamagiwa M 2011 J. Nucl. Mater. 418 152
[20]	Xia M, Guo H Y, Dai Y, Yan Q Z, Guo L P, Li T C, Qiao Y, Ge C C 2014 Chin. Phys. B 23 127806

施引文献

[1]	Hao J K 2007 Fusion Reactor Material (Beijing: Chemical Industry Press) p12 (in Chinese) [郝嘉琨 2007 聚变堆材料 (北京: 化学工业出版社)第12页]
[2]	Xia M, Yan Q Z, Xu L, Guo H Y, Zhu L X, Ge C C 2013 J. Nucl. Mater. 434 85
[3]	Xia M, Yan Q Z, Xu L, Zhu L X, Guo H Y, Ge C C 2013 J. Nucl. Mater. 430 216
[4]	Andreani R, Diegele E, Laesser R, van der Schaaf B 2004 J. Nucl. Mater. 329-333 20
[5]	Morenzo B, Edgar B, Karin B, Luigi D P, Robin F, Luciano G, Stephan H, Claudio N, Prachai N, Aldo P, Neill T, David W 2005 Fusion Eng. Des. 75-79 1173
[6]	Maisonnier D, Cook I, Pierre S, Lorenzo B, Luigi D P, Luciano G, Prachai N, Aldo P 2006 Fusion Eng. Des. 81 1123
[7]	Lässer R, Baluc N, Boutard J L, Diegele E, Dudarev S, Gasparotto M, Möslang A, Pippan B, Riccardi B, van der Schaaf B 2007 Fusion Eng. Des. 82 511
[8]	Linke J, Akiba M, Bolt H, Breitbach G, Duwe R, Makhankov A, Ovchinnikov I, Rödig M, Wallura E 1997 J. Nucl. Mater. 241-243 1210
[9]	Singheiser L, Hirai T, Linke J, Pintsuk M, Rödig M 2009 Trans. Indian Inst. Metals. 62 123
[10]	Philipps V 2011 J. Nucl. Mater. 415 S2
[11]	Song B, Guo L P, Li M, Li C J, Ye M S, Fu D J, Fan X J 2007 Nuclear Techniques 30 777 (in Chinese) [宋搏, 郭立平, 黎明, 李传佳, 叶明生, 付德军, 范湘军 2007 核技术 30 777]
[12]	Yu J N, Sha J J, Yu G 2013 Proceedings of the 16th International Conference on Fusion Reactor Materials (ICFRM-16) Beijing, China, October 20-26, 2013
[13]	Ziegler J F, Biersack J P, Littmark U 1985 Ion Implantation Science and Technology (New York: Academic Press) p51
[14]	Wang T Q, Shen Y P, Zhang R Q, Wang S W, Zhang S F 2000 High Power Laser and Particle Beams 12 339 (in Chinese) [王同权, 沈永平, 张若棋, 王尚武, 张树发 2000 强激光与粒子束 12 339]
[15]	Wang P X, Song J S 2002 Material of Helium and Tritium Permeation (Beijing: National Defence Industry Press) p30 (in Chinese) [王佩璇, 宋家树 2002 材料中的氦及氚渗透(北京: 国防工业出版社) 第30页]
[16]	Hartley F R 1973 The Chemistry of Platinum and Palladium: with Particular Reference to Complexes of the Elements (London:Applied Science Publishers) p5334
[17]	Kajita S, Sakaguchi W, Ohno N, Yoshida N, Saeki T 2009 Nucl. Fusion 49 95005
[18]	Cipiti B B, Kulcinski G L 2005 J. Nucl. Mater. 347 298
[19]	Kajita S, Yoshida N, Yoshihara R, Ohno N, Yamagiwa M 2011 J. Nucl. Mater. 418 152
[20]	Xia M, Guo H Y, Dai Y, Yan Q Z, Guo L P, Li T C, Qiao Y, Ge C C 2014 Chin. Phys. B 23 127806

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