SQUID法和Campbell法测量超导材料的研究

郭志超; 索红莉; 刘志勇; 刘敏; 马麟

doi:10.7498/aps.61.177401

摘要

本文对比研究了超导材料磁测量中的SQUID法和Campbell法; 并用高压PIT法制备的超导材料MgB2作为测量样品,用两种方法,测量了超导样品的临界电流密度, 分别得到了样品的Jc-B关系曲线; SQUID法测量样品的外磁场可以达到6 T, 此时材料已经处于失超状态,此方法测得的结果是样品各个小区域结果的平均值, SQUID还可以用来进一步标度材料的钉扎力行为,研究材料磁特性. Campbell法测量只能测量到外磁场强度为0.4 T,外磁场的交流部分的频率可以达到800 Hz, 用这种测量方法得到的是整块样品的电流,由于测量计及材料内部微观结构缺陷等影响电流传输因素, 所测结果小于直流磁化法,但更切近材料实际电流,能用来深入研究材料内部结构差别对材料电性能的影响.

关键词:

Abstract

The two magnetic measurement methods of superconductors, SQUID method and Campbell method, are introduced briefly. Superconducting properties of MgB2 bulk samples are prepared by the high-pressure powder in tube (PIT) sintering method. The two measurement methods are employed to measure the critical current density of the sample. The Jc-B curves of the MgB2 samples are obtained with each method. The SQUID method can be used to measure the magnetic strength field up to 6 T and the material is in normal state, and the result is used to scale F(b) of the pinning through necessary calculation which is used to study the magnetic characteristic of the material. The critical current density (Jc) measured by the SQUID method is the average of the materials different parts. Jc is measured and estimated by the Campbell's method. The magnetic field is only to 0.4 T while the frequency of the AC parts magnetic field is varied from 37 Hz to 797 Hz. The critical current density obtained by Campbell's method is smaller than that obtained by the SQUID measurement, which is due to the existence of various faults and the decrease of the electrical connectivity.

Keywords:

SQUID method /
Campbell method /
superconductivity critical current density

作者及机构信息

1.
北京工业大学材料学院, 国家教育部功能材料重点实验室, 北京 100124

基金项目: 国家重点基础研究发展计划(973计划) (批准号: 2006CB601005); 国家高技术研究发展计划(863)项目(批准号: 2009AA032401); 国家自然科学基金(批准号: 50771003和50802004) 和北京市自然科学基金(批准号: 2092006)资助的课题.

Authors and contacts

1.
The Key Laboratory of Advanced Functional Materials, Ministry of Education, College of Materials Science and Engineering, Beijing University of Technology, Beijing 100124, China

Funds: Project supported by the National Basic Research Program 973 of China (Grant No. 2006CB601005), the National High Technology Research and Development Program 863 of China (Grant No. 2009AA032401), the National Natural Science Foundation of China (Grant Nos. 50771003 and 50802004), and the Beijing Municipal Natural Science Foundation (Grant No. 2092006).

参考文献

[1]	Gumbel A, Eckert J, Fucks G 2002 Appl. Phys. Lett. 80 2725
[2]	Kosse A I, Prokhorov A Y, Khokhlov V A 2008 Supercond. Sci. Technol. 21 075015
[3]	Teruo M 2007 Flux pinning in superconductors (Berlin: Springer-Verlag) p221
[4]	Gallitto A A, Bonsignore G, Giunchi G, Vigni M L 2007 J. Supercond. Nov. Magn. 20 13
[5]	Zheng D N, Campbell A M, Johnson J D, Cooper J R, Blunt F J 1994 Phys. Rev. B 49 1417
[6]	Ni B, Liu Z Y, Yoshihiro M 2008 Phys. C 468 1443
[7]	Huan Y, Luo H Q, Wang Z S 2008 Appl. Phys. Lett. 93 142506
[8]	Campbell A M 1969 Phys. C: Solid State Phys. 2 1492
[9]	Bean C P 1962 Phys. Rev. Lett. 8 250
[10]	Lodon H 1963 Phys. Lett. 6 162
[11]	Yasukoch K, Ogasawara T, Ushino N 1964 Phys. Soc. Jpn. 19 1649
[12]	Jin H L, Jin X, Fang H C 1992 Chin. J. Low Temp. Phys. 14 12 (in Chinese) [吉和林, 金新, 范宏昌 1992 低温 14 12]
[13]	Otabe E S, Ohtani N, Matsushita T, Ishikawa Y, Yoshizawa S 1994 Jpn. J. Appl. Phys. 33 996
[14]	Wang R F, Zhao S P, Xu F Z 2002 Acta Phys. Sin. 51 889 (in Chinese) [王瑞峰, 赵士平, 徐凤枝 2002 51 889]
[15]	Kimishima Y, Takami S, Okuda T 2007 Phys. C 463 281
[16]	Kulich M, Kovac P, Weber H W 2011 Supercond. Sci. Technol. 24 065025
[17]	He L, Hu X, Yin L 2009 Acta Phys. Sin. 58 417 (in Chinese) [贺丽, 胡翔, 尹澜 2009 58 417]
[18]	Chu H F, Li J, Li S 2010 Acta Phys. Sin. 59 6585 (in Chinese) [储海峰, 李洁, 李绍, 黎松林 2010 59 6585]

施引文献

[1]	Gumbel A, Eckert J, Fucks G 2002 Appl. Phys. Lett. 80 2725
[2]	Kosse A I, Prokhorov A Y, Khokhlov V A 2008 Supercond. Sci. Technol. 21 075015
[3]	Teruo M 2007 Flux pinning in superconductors (Berlin: Springer-Verlag) p221
[4]	Gallitto A A, Bonsignore G, Giunchi G, Vigni M L 2007 J. Supercond. Nov. Magn. 20 13
[5]	Zheng D N, Campbell A M, Johnson J D, Cooper J R, Blunt F J 1994 Phys. Rev. B 49 1417
[6]	Ni B, Liu Z Y, Yoshihiro M 2008 Phys. C 468 1443
[7]	Huan Y, Luo H Q, Wang Z S 2008 Appl. Phys. Lett. 93 142506
[8]	Campbell A M 1969 Phys. C: Solid State Phys. 2 1492
[9]	Bean C P 1962 Phys. Rev. Lett. 8 250
[10]	Lodon H 1963 Phys. Lett. 6 162
[11]	Yasukoch K, Ogasawara T, Ushino N 1964 Phys. Soc. Jpn. 19 1649
[12]	Jin H L, Jin X, Fang H C 1992 Chin. J. Low Temp. Phys. 14 12 (in Chinese) [吉和林, 金新, 范宏昌 1992 低温 14 12]
[13]	Otabe E S, Ohtani N, Matsushita T, Ishikawa Y, Yoshizawa S 1994 Jpn. J. Appl. Phys. 33 996
[14]	Wang R F, Zhao S P, Xu F Z 2002 Acta Phys. Sin. 51 889 (in Chinese) [王瑞峰, 赵士平, 徐凤枝 2002 51 889]
[15]	Kimishima Y, Takami S, Okuda T 2007 Phys. C 463 281
[16]	Kulich M, Kovac P, Weber H W 2011 Supercond. Sci. Technol. 24 065025
[17]	He L, Hu X, Yin L 2009 Acta Phys. Sin. 58 417 (in Chinese) [贺丽, 胡翔, 尹澜 2009 58 417]
[18]	Chu H F, Li J, Li S 2010 Acta Phys. Sin. 59 6585 (in Chinese) [储海峰, 李洁, 李绍, 黎松林 2010 59 6585]

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